Analysis of acetyltributyl citrate's migration from PVC in oily simulant by GC/MS

China Brewing ›› 2012, Vol. 31 ›› Issue (9) : 162-165.

PDF(326 KB)
PDF(326 KB)
China Brewing ›› 2012, Vol. 31 ›› Issue (9) : 162-165.

Analysis of acetyltributyl citrate's migration from PVC in oily simulant by GC/MS

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Abstract

A method was established to determine migration of plasticizer ATBC of PVC sealed gaskets in oily simulant. The plasticizer ATBC was ultrasonic extracted and using n-hexane as the oily simulant. Qualitative and quantitative analysis of ATBC was carried out by GC/MS. The method has a good relationship at the range of 1ml/L~200ml/L, with correlation coefficients 0.9973. In the tests of accuracy and precision, the average recovery was 95.8%~105.2%, and the relative standard deviation(RSD) was 1.03%~4.72%.This method can provide some references for studying the migration of citrate plasticizers in oily food.

Key words

GC/MS / PVC / migration / plasticizers

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Analysis of acetyltributyl citrate's migration from PVC in oily simulant by GC/MS[J]. China Brewing, 2012, 31(9): 162-165
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